Pb(II)

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Synthesis of 1-(Furan-2-yl) imine Functionalized Silica as a Chelating Sorbent and its Preliminary Use in Metal Ion Adsorption

Journal Title, Volume, Page: 
Separation Science and Technology. 11/2014; 49(17):xxxx-xxxx
Year of Publication: 
2014
Authors: 
Said TIGHADOUINI
LCAE, Faculté des Sciences, Université Mohamed I, 60 000 Oujda, Morocco
Smaail RADI
LCAE, Faculté des Sciences, Université Mohamed I, 60 000 Oujda, Morocco
Maryse BACQUET
Université des Sciences et Technologies de Lille, UMET: Unité Matériaux et Transformations UMR8207, Equipe Ingénierie des Systèmes Polymères, Bâtiment C6 salle 119-59655 Villeneuve d’Ascq, France
Jean-Philippe DACQUIN
Unité de Catalyse et Chimie du Solide, CNRS 8181, Université Lille 1, 59655 Villeneuve d’Ascq, France
Yahia Nasser MABKHOT
Department of Chemistry, Faculty of Science, King Saud University, P. O. Box 2455, Riyadh 11451, Saudi Arabia
Shehdeh JODEH
Department of Chemistry, Faculty of Science, An-Najah National University, Nablus, Palestine
Current Affiliation: 
Department of Chemistry, Faculty of Science, An-Najah National University, Nablus, Palestine
Preferred Abstract (Original): 

A new silica gel material covalently bonded with 1-(furan-2-yl) imine (SiNFn) was synthesized and well characterized by elemental analysis, FT-IR, 13C NMR of the solid state, nitrogen adsorption-desorption isotherm, BET surface area, B.J.H. pore sizes, thermogravimetry analyser (TGA) curves, and scanning electron microscope (SEM). The new chelating surface exhibits good chemical and thermal stability. The synthesized SiNFn was investigated as an adsorbent for removal of Cu(II), Zn(II), Cd(II) and Pb(II) from aqueous solution. The determination of metal ions was carried out on FAAS using batch method. The adsorption capacity was investigated using kinetics and pH effects. The preliminary results show that the new material present high adsorption toward copper compared to others described sorbents.

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Synthesis of 1-(Furan-2-yl) imine Functionalized Silica as a Chelating Sorbent and its Preliminary Use in Metal Ion Adsorption

Journal Title, Volume, Page: 
Separation Science and Technology. 11/2014; 49(17):xxxx-xxxx
Year of Publication: 
2014
Authors: 
Said TIGHADOUINI
LCAE, Faculté des Sciences, Université Mohamed I, 60 000 Oujda, Morocco
Smaail RADI
LCAE, Faculté des Sciences, Université Mohamed I, 60 000 Oujda, Morocco
Maryse BACQUET
Université des Sciences et Technologies de Lille, UMET: Unité Matériaux et Transformations UMR8207, Equipe Ingénierie des Systèmes Polymères, Bâtiment C6 salle 119-59655 Villeneuve d’Ascq, France
Jean-Philippe DACQUIN
Unité de Catalyse et Chimie du Solide, CNRS 8181, Université Lille 1, 59655 Villeneuve d’Ascq, France
Yahia Nasser MABKHOT
Department of Chemistry, Faculty of Science, King Saud University, P. O. Box 2455, Riyadh 11451, Saudi Arabia
Shehdeh JODEH
Department of Chemistry, Faculty of Science, An-Najah National University, Nablus, Palestine
Ismail WARAD
Department of Chemistry, Faculty of Science, An-Najah National University, Nablus, Palestine
Current Affiliation: 
Department of Chemistry, Faculty of Science, An-Najah National University, Nablus, Palestine
Mustapha ZAGHRIOUI
Department of Chemistry, Faculty of Science, An-Najah National University, Nablus, Palestine
Preferred Abstract (Original): 

A new silica gel material covalently bonded with 1-(furan-2-yl) imine (SiNFn) was synthesized and well characterized by elemental analysis, FT-IR, 13C NMR of the solid state, nitrogen adsorption-desorption isotherm, BET surface area, B.J.H. pore sizes, thermogravimetry analyser (TGA) curves, and scanning electron microscope (SEM). The new chelating surface exhibits good chemical and thermal stability. The synthesized SiNFn was investigated as an adsorbent for removal of Cu(II), Zn(II), Cd(II) and Pb(II) from aqueous solution. The determination of metal ions was carried out on FAAS using batch method. The adsorption capacity was investigated using kinetics and pH effects. The preliminary results show that the new material present high adsorption toward copper compared to others described sorbents.


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