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diphenyl pyraline hydrochloride

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Crystal Structure of Diphenyl Pyraline Hydrochloride-Cobalt Chloride Complex

Wed, 2014-02-26 14:05 — Dr. Muneer Mustafa Mahd Abdoh
Journal Title, Volume, Page: 
Mol. Cryst. Liq. Cryst, 1994, Vol. 250, 285- 291
Year of Publication: 
1994
Link: 
http://www.tandfonline.com/doi/abs/10.1080/10587259408028213?journalCode=gmcl19
Authors: 
M. M. M. Abdoh
Department of Studies in Physics , University of Mysore , Manasagangothri, Mysore, 570006, India
Current Affiliation: 
Department of Physics, Faculty of Science, An-Najah National University, Nablus, Palestine
[email protected]
M. A. Sridhar
Department of Studies in Physics , University of Mysore , Manasagangothri, Mysore, 570006, India
A. Indira
Department of Studies in Physics , University of Mysore , Manasagangothri, Mysore, 570006, India
S. B. Bellad
Department of Studies in Physics , University of Mysore , Manasagangothri, Mysore, 570006, India
A. M. Babu
Department of Studies in Physics , University of Mysore , Manasagangothri, Mysore, 570006, India
J. S. Prasad
Department of Studies in Physics , University of Mysore , Manasagangothri, Mysore, 570006, India
P. G. Ramappa
Department of Studies in Chemistry , University of Mysore , Manasagangothri, Mysore, 570006, India
K. G. Somasekharappa
Department of Studies in Chemistry , University of Mysore , Manasagangothri, Mysore, 570006, India
Preferred Abstract (Original): 

The crystal structure of the complex of diphenyl pyraline hydrochloride with cobalt chloride, C38H46O2N2Cl4Co has been determined by X-ray diffraction using CuKα radiation. The compound crystallizes in monoclinic space group P21/n with the cell parameters a = 18.120(4)Å, b = 8.179(3)Å, c = 26.805(3)Å, β = 102.60(1)° with Z = 4, V = 3876(1)Å3. The structure was solved using 5484 reflections. The stucture was refined to a final wR of 0.2944 (R = 0.1130). The packing of the molecules shows a layered arrangement.

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