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Assignment of the 13C-NMR Spectrum of Phenanthro[4,3-A]dibenzothiophene Through the Uatilization of two-dimensional Relayed Coherence Transfer and Double Quantum Coherence Spectroscopy

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Sun, 2014-01-26 11:57 — Mohammad Musmar
Journal Title, Volume, Page: 
Journal of Heterocyclic Chemistry Volume 22, Issue 1, pages 219–223, January/February 1985
Year of Publication: 
1985
Link: 
http://onlinelibrary.wiley.com/doi/10.1002/jhet.5570220152/abstract
Authors: 
M. J. Musmar
Department of Medicinal Chemistry, College of Pharmacy, University of Houston, Houston, Texas 77004
Current Affiliation: 
Department of Pharmacy, Faculty of Medicine and Health Sciences, An-Najah National University, Nablus, Palestine
[email protected]
Gary E. Martin
Department of Medicinal Chemistry, College of Pharmacy, University of Houston, Houston, Texas 77004
Robert T. Gampe Jr.
Department of Biochemistry and Molecular Biology, University of Texas, Health Science Center, Houston, Texas
Milton L. Lee
Department of Chemistry, Brigham Young University, Provo, Utah 84602
Ralph E. Hurd
General Electric NMR, 255 Fourier Avenue, Freemont, California 94539
Marvin L. Tedjamulia
Department of Chemistry, University of South Florida, Tampa, Florida 33620
Hirotaka Kudo
Department of Chemistry, University of South Florida, Tampa, Florida 33620
Raymond N. Castle
Preferred Abstract (Original): 

Total assignment of the 13C-nmr spectrum of the helical molecule phenanthro[4,3-a]dibenzothiophene at 125.762 MHz is reported. Assignments were made by the combined application of 13C-13C autocorrelated double quantum coherence and heteronuclear relayed coherence transfer (RELAY) experiments.

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Assignment_of_the_13C-NMR_Spectrum_of_Phenanthro[4,3-A]dibenzothiophene_Through_the_Uatilization_of_two-dimensional_Relayed_Coherence_Transfer_and_Double_Quantum_Coherence_Spectroscopyا.pdf1.12 MB